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Black spruce absolute

Vân sam đen absolute

Picea mariana (Mill.) Britton, Sterns & Poggenb.

Spruce needle absolute, Épinette noire absolute

Pinaceae · Lá kim và cành non · Needles and young twigs · Solvent-extracted (concrete, absolute)


Aroma

Deep green needles, balsamic resin, damp wood. Less camphoraceous than the oil. A softly sweet base with hints of jammy fruit and leather.


Safety

The IFRA standard "Pinacea derivatives" (specification, 1994) applies to materials from the pine family: they should only be used with peroxide levels kept as low as practicable, for example by adding antioxidants at production.

α-Pinene, β-pinene and limonene, common in pine family materials, are on the EU fragrance allergen list. They must be labelled above 0.001 percent in leave-on or 0.01 percent in rinse-off products.

Oxidised terpenes can form sensitising products. Store dark, sealed and cool with minimal headspace.


Usage guidelines

Note
Heart
Form
Absolute; the distilled oil is more common
Role
Deep conifer note for fougère, chypre, forest accords
Limits
Peroxide specification (IFRA, pine family)
Storage
Dark, sealed, cool

Chemistry

Key constituents
Bornyl acetatemajor in the distilled oil
Camphenemajor in the distilled oil
α-Pinenemajor in the distilled oil
δ-3-Carenepresent
Limonenepresent

Origins

Canada


Notes

Black spruce is a conifer of the North American boreal forest, ranging from Alaska across Canada to the Great Lakes. The steam-distilled needle oil already has its own page in the library. The absolute is the solvent-extracted form and is less common.

Extraction has two steps. Needles and twigs are extracted with a non-polar solvent to give a concrete. The concrete is washed with ethanol, chilled to remove waxes and freed of alcohol to give the absolute.

Compared with the oil, the absolute keeps more heavy matter: diterpenes, resin acids, pigments and residual waxes. Its odour is rounder, less camphoraceous and slower to evaporate.

The composition of black spruce oil is well studied: bornyl acetate, camphene and α-pinene lead. Data specific to the absolute are rarely published; the supplier's certificate of analysis is the reference.

In perfumery, black spruce absolute gives a dark conifer note for fougères, chypres and forest accords. It links well with labdanum, cedarwood and leather notes.

As a pine family material, the absolute falls under the IFRA peroxide specification. Storage conditions decide how stable a lot remains.


Sources

  1. IFRA Standards, 51st Amendment: Index of IFRA Standards (notified 30 June 2023)
  2. Commission Regulation (EU) 2023/1545 amending Reg. 1223/2009 on labelling of fragrance allergens
  3. The Good Scents Company Information System: spruce needle absolute
  4. Plants of the World Online, Royal Botanic Gardens Kew (accepted names)
  5. Tisserand R., Young R. Essential Oil Safety, 2nd ed., Churchill Livingstone, 2014